Steklo i Keramika (Glass and Ceramics). Monthly scientific, technical and industrial journal

 

ISSN 0131-9582 (Online)

  • Continuous numbering: 1065
  • Pages: 23-27
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The effect of ultrasonic treatment (22 kHz) of a suspension of metakaolin, aluminum oxide and sodium hydroxide at a molar ratio Al 2 O 3 2SiO 2 : NaOH: Al 2 O 3 = 6: 12: 2 with subsequent heat treatment and hydrothermal crystallization for the synthesis of LTA zeolite. It has been established that an increase in the S: L ratio at the stage of ultrasonic treatment makes it possible to increase the yield of the target product. The optimal conditions for ultrasonic treatment were determined (amplitude 8 ?m, time about 10 min). It has been shown that under optimal conditions the degree of crystallinity of the LTA zeolite is 98%. A comparison of the regularities of the synthesis of LTA zeolite using ultrasonic treatment and mechanochemical activation is given.
Cand. tech. Sciences N.E. Gordin ( e-mail: This email address is being protected from spambots. You need JavaScript enabled to view it. ), Dr. Sci. V. Yu. Prokofiev ( e-mail: This email address is being protected from spambots. You need JavaScript enabled to view it. ), Yu. N. Kulpina, N. V. Petukhova, S. I. Gazakhova, O. E. Khmylova; Research Institute of Thermodynamics and Kinetics of Chemical Processes, Ivanovo State University of Chemical Technology (Russia, Ivanovo)
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Gordina N. E., Prokofiev V. Yu., Kul?pina Yu. N., Petukhova N. V., Gazakhova S. I., Khmylova O. E. The use of ultrasonic processing in early-stage synthesis of LTA zeolite from metakaoline. Steklo i keramika. 2016:89(9):23-27. (in Russ). UDK 661.183.6:54.056