Steklo i Keramika (Glass and Ceramics). Monthly scientific, technical and industrial journal

 

ISSN 0131-9582 (Online)

  • Continuous numbering: 1009
  • Pages: 30-36
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Heading: Biomaterials

Calcium hydroxyapatite (HAP) powder is synthesized from an aqueous solution of potassium hydrogen phosphate and a suspension of calcium hydroxide in an aqueous solution containing calcium and potassium ions, hydroxide ions and acetate ions. The amount of Ca (OH) 2 in the calcium-containing component was 50, 75 and 100%. The synthesized HAP powder was used to obtain ceramics. Ceramics after firing at 700 ° C from HAP powder containing a by-product of the reaction had a density of 2.0 - 2.6 g / cm 3 and a flexural strength of 35 - 45 MPa at a grain size of 200 nm. The phase composition was represented by HAP and double calcium orthophosphate of potassium. Ceramics based on HAP, after firing at 1200 ° C from a powder that does not contain a by-product of the reaction, had a density of 2.2 - 2.3 g / cm 3 and a flexural strength of 45 - 55 MPa at a grain size 500 - 1000 nm. Tab. 2, ill. 11, bibliography: 14 titles.
Safronova T.V., Shekhirev M.A., Putlyaev V.I., Tretyakov Yu.D. Ceramic materials based on hydroxyapatite synthesized from solutions of various concentrations // Inorganic Materials. 2007. N 8.S. 1005-1014. Pretto M., Costa AL, Landi E. et al. Dispersing behavior of hydroxyapatite powders produced by wet-chemical synthesis // J. Am. Ceram. Soc. 2003. V. 86. N 9. P. 1534 - 1539. Safronova T. V., Steklov M. Yu., Putlyaev V. I., Shekhirev M. A. Na-substituted Ca-deficient carbonate hydroxyapatite for the production of ceramic materials / / Structures made of composite materials. 2006. N 4. S. 39-43. Donadel K., Laranjeira Mauro CM, Gonzalves VL et al. Hydroxyapatites produced by wet-chemical methods // J. Am. Ceram. Soc. 2005. V. 88. N 8. P. 2230 - 2235. Safronova TV Phase composition of ceramics based on calcium hydroxyapatite powders containing by-products of the synthesis reaction // Glass and ceramics. 2009. N4. S. 21-24. Safronova TV Phase composition of ceramics based of powders calcium hydroxyapatite containing synthesis byproducts // Glass and Ceramics. 2009. V. 66. No. 3-4. P. 136-139. Safronova T.V., Korneichuk S.A., Putlyaev V.I., Boytsova O.V. Ceramics based on calcium hydroxyapatite synthesized from calcium acetate and potassium hydrogen phosphate // Glass and ceramics. 2008. N 4. S. 19 - 24. Safronova TV, Korneichuk SA, Putlayev VI, Boitsova OV Ceramic made from calcium hydroxyapatite synthesized from calcium acetate and potassium hydrophosphate // Glass and Ceramics. 2008. V. 65. No. 3 - 4. P. 131 - 135. Spiridonov Yu. A., Orlova LA Problems of foam glass production // Glass and ceramics. 2003. N 10.S. 10-11. Spiridonov Yu. A., Orlova LA Problems of foam glass production // Glass and Ceramic. 2003. V. 60. No. 9-10. Suetsugu Y., Shimoya I., Tanaka J. Configuration of carbonate ions in apatite structure // J. Am. Ceram. Soc. 1998. V. 81. N3. P. 746-748. Hattori T., Lwadate Ya. Hydrothermal preparation of calcium hydroxyapatite powders // J. Am. Ceram. Soc. 1990. V. 73. N6. P. 1803-1805. Orlovsky V.P., Kurdyumov S.G., Slivko OI Synthesis, properties and application of calcium hydroxyapatite // Dentistry. 1996. T. 75. N 5. S. 68 - 73. Larionov D., Putlyaev V., Kuznetsov A., Veresov A. Different approaches to fabrication of bulk biomaterials based on calcium phosphates // Program and Book of abstructs: The Eighth Students' Meeting - SM-2009 Processing and Application of Ceramics, Novi Sad, December 2-5, 2009. Vlasova EB, Beletskiy BN Hydroxyapatite for bioactive glass ceramics // Inorganic materials. 1992. T. 28. N 9.S. 1936-1939. Stepuk A. A., Veresov A. G. Putlyaev V. P., Tretyakov Yu. D. Effect of NO, CH3COO "and SG ions on the morphology of calcium hydroxyapatite crystals // Reports of the Academy of Sciences. 2007. Vol. 412. No. 2. P. 211 - 215. Phase equilibria diagrams database // ACerS-NINST.

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T. V. Safronova, S. A. Korneichuk, V. I. Putlyaev, and V. K. Krut'ko Ceramics based on hydroxyapatite calcium, synthesized from calcium acetate, calcium hydroxide, and dipotassium phosphate. Steklo i keramika. 2012:85(1):30-36. (in Russ). UDK 666.3:546.41'18