Composite bioceramics with a density of at least 80% of the theoretical was obtained from thermolyzed octacalcium phosphate (OCP). OCP processing temperatures were 450, 600, and 700 ° C. Ceramics were obtained by firing thermolyzed powders at a maximum temperature of 1000, 1050, and 1100 ° C with holding for 3, 6 and 9 h. The highest strength characteristics (up to 125 MPa when measuring the flexural strength) are demonstrated by samples obtained from OCP treated at 450
Sarkisov PD, Mikhailenko N. Yu. Bioactive inorganic materials for bone endoprosthetics // Tekhnika i tekhnologiya silikatov. 1994. T. 1.? 2.S. 5? 11.
Putlyaev VI, Safronova TV New generation of calcium phosphate biomaterials: the role of phase and chemical composition // Glass and ceramics. 2006.? 3.S. 30? 33.
? Putlyaev VI, Safronova TV A new generation of calcium phosphate biomaterials: the role of phase and chemical compositions // Glass and Ceram. 2006. V. 63. N 3? 4. P. 99? 102.?
Veresov A.G., Putlyaev V.I., Tretyakov Yu. D. Advances in the field of calcium phosphate biomaterials // Russian Chemical Journal. 2000. T. XLIV. ? 6. Part II. C. 32? 46.
Barinov SM, Komlev VS Bioceramics based on calcium phosphates. Moscow: Nauka, 2005.204 p.
Suchanek W., Yoshimura M. Processing and properties of hydroxyapatite-based biomaterials for use as hard tissue replacement implants // J. Mater. Res. 1998. V. 13. N 1. P. 94? 117.
Goldberg MA, Smirnov VV, Kutsev SV et al. Composite ceramic materials of the hydroxyapatite system? calcium carbonate // Inorganic materials. 2010.Vol. 46.? 11, p. 1397? 1402.
Otsuka M., Marunaka S., Matsuda Y. et al. Calcium level-responsive in-vitro zinc release from zinc containing tricalcium phosphate (ZnTCP) // J. Biomed. Mater. Res. 2000. V. 52. P. 819? 824.
Barralet J., Best S., Bonfield W. Carbonate substitution in precipitated hydroxyapatite: An investigation into the effects of reaction temperature and bicarbonate ion concentration // J. Biomed. Mater. Res. 1998. V. 41. P. 79? 86.
Safronova TV, Knot'ko AV, Shatalova TB et al. Ceramics based on calcium phosphates from a powder synthesized from a mixed-anionic solution // Glass and ceramics. 2016.? 1.P. 27? 34.
? Safronova TV, Knot? Ko AV, Shatalova TBet al. Calcium phosphate ceramic based on powder synthesized from a mixed-anionic solution // Glass and Ceram. 2016. V. 73. N 1? 2. P. 25? 31.?
Safronova T.V., Putlyaev V.I., Shekhirev M.A., Kuznetsov A.V. Composite ceramics containing a bioresorbable phase // Glass and ceramics. 2007.? 3.S. 31? 35.
? Safronova TV, Putlyaev VI, Shekhirev MA, Kuznetsov AV Composite ceramic containing a bioresorbable phase // Glass and Ceram. 2007. V. 64.? 3? 4. P. 102? 106.?
Kanazawa T. Inorganic phosphate materials: trans. with jap. Kiev: Naukova Dumka, 1998.298 p.
Sakamoto K., Yamaguchi S., Kaneno M. et al. Synthesis and thermal decomposition of layered calcium phosphates including carboxylate ions // Thin Solid Films. 2008. V. 517. N 4. P. 1354? 1357.
Pat. 245653 RF, IPC A61L 27/12, IPC B82B 3/00, IPC C04B 35/447. Method of preparing a charge for obtaining ceramic biodegradable material / V. I. Putlyaev, T. V. Safronova, E. V. Kukueva, Yu. D. Tretyakov; publ. 20.07.2012.
Putlyaev VI, Kukueva EV, Safronova TV et al. Features of octacalcium phosphate thermolysis // Refractories and Industrial Ceramics. 2014. V. 54. N 5. P. 420? 424.
Deville S., Saiz E., Nalla RK, Tomsia AP Freezing as a Path to Build Complex Composites // Science. 2006. V. 3. N 11. P. 515? 518.
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